di-tert-butyl (3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)methyl phosphate

Base Information

Chemical Name:di-tert-butyl (3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)methyl phosphate
CAS No.:1340480-33-2
Molecular Formula:C₂₉H₃₀ClF₃N₅O₆P
Molecular Weight:668.009
Hs Code.:

Synonyms:di-tert-butyl (3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)methyl phosphate

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Chemical Property of di-tert-butyl (3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)methyl phosphate

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Technology Process of di-tert-butyl (3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)methyl phosphate

There total 2 articles about di-tert-butyl (3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)methyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1155846-67-5
3-chloro-5-{[2-oxo-1-(1H-pyrazolo[3,4-b]pyridin-3-ylmethyl)-4-(trifluoromethyl)-1,2-dihydropyridin-3-yl]oxy}benzonitrile

: 229625-50-7
di-tert-butyl chloromethyl phosphate

: 1340480-33-2
di-tert-butyl (3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)methyl phosphate

Guidance literature:: With caesium carbonate; In ISOPROPYLAMIDE; at 20 - 25 ℃; for 23h; Inert atmosphere;

Reference yield:

: barium bis(di-tert-butyl phosphate)

: 1340480-33-2
di-tert-butyl (3-{[3-(3-chloro-5-cyanophenoxy)-2-oxo-4-(trifluoromethyl)pyridin-1(2H)-yl]methyl}-1H-pyrazolo[3,4-b]pyridin-1-yl)methyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / tetra(n-butyl)ammonium hydrogensulfate / dichloromethane; water / 16.5 h / 0 - 25 °C / Inert atmosphere

2: caesium carbonate / ISOPROPYLAMIDE / 23 h / 20 - 25 °C / Inert atmosphere

With sodium carbonate; caesium carbonate; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; ISOPROPYLAMIDE; water;