Technology Process of 6-Phthalazinamine (9CI)
There total 3 articles about 6-Phthalazinamine (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium tetrahydroborate; boron trifluoride diethyl etherate / 1,2-dimethoxyethane
2: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane
3: hydrazine hydrate / dichloromethane; ethanol
4: hydrogen; palladium 10% on activated carbon / methanol
With
sodium tetrahydroborate; oxalyl dichloride; palladium 10% on activated carbon; boron trifluoride diethyl etherate; hydrogen; hydrazine hydrate; dimethyl sulfoxide; triethylamine;
In
methanol; 1,2-dimethoxyethane; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2014.12.086
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride; triethylamine; dimethyl sulfoxide / dichloromethane
2: hydrazine hydrate / dichloromethane; ethanol
3: hydrogen; palladium 10% on activated carbon / methanol
With
oxalyl dichloride; palladium 10% on activated carbon; hydrogen; hydrazine hydrate; dimethyl sulfoxide; triethylamine;
In
methanol; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2014.12.086
