(3S,5R,7R)-5-O-(4-methoxybenzyl)-7-O-tert-butyldimethylsilyl-1-(4-tert-butyldimethylsilyloxyphenyl)octadecane-3,5,7-triol

Base Information

Chemical Name:(3S,5R,7R)-5-O-(4-methoxybenzyl)-7-O-tert-butyldimethylsilyl-1-(4-tert-butyldimethylsilyloxyphenyl)octadecane-3,5,7-triol
CAS No.:1206482-52-1
Molecular Formula:C₄₄H₇₈O₅Si₂
Molecular Weight:743.271
Hs Code.:

Synonyms:(3S,5R,7R)-5-O-(4-methoxybenzyl)-7-O-tert-butyldimethylsilyl-1-(4-tert-butyldimethylsilyloxyphenyl)octadecane-3,5,7-triol

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Chemical Property of (3S,5R,7R)-5-O-(4-methoxybenzyl)-7-O-tert-butyldimethylsilyl-1-(4-tert-butyldimethylsilyloxyphenyl)octadecane-3,5,7-triol

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Technology Process of (3S,5R,7R)-5-O-(4-methoxybenzyl)-7-O-tert-butyldimethylsilyl-1-(4-tert-butyldimethylsilyloxyphenyl)octadecane-3,5,7-triol

There total 1 articles about (3S,5R,7R)-5-O-(4-methoxybenzyl)-7-O-tert-butyldimethylsilyl-1-(4-tert-butyldimethylsilyloxyphenyl)octadecane-3,5,7-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1206482-51-0
((3R,5R,7R)-3-(benzyloxy)-1-(4-(tert-butyldimethylsilyloxy)phenyl)-5-(4-methoxybenzyloxy)octadeca-1,9-diyn-7-yloxy)(tert-butyl)dimethylsilane

: 1206482-52-1
(3S,5R,7R)-5-O-(4-methoxybenzyl)-7-O-tert-butyldimethylsilyl-1-(4-tert-butyldimethylsilyloxyphenyl)octadecane-3,5,7-triol

Guidance literature:: With hydrogen; nickel; In ethanol; at 20 - 55 ℃; for 24h; under 1034.32 Torr; regioselective reaction;
DOI:10.1016/j.tet.2009.10.058

Reference yield: 95.0%

: 1206482-52-1
(3S,5R,7R)-5-O-(4-methoxybenzyl)-7-O-tert-butyldimethylsilyl-1-(4-tert-butyldimethylsilyloxyphenyl)octadecane-3,5,7-triol

: 1206482-53-2
(5S,7R)-5-(4-methoxybenzyloxy)-7-(tert-butyldimethylsilyloxy)-1-(4-tert-butyldimethylsilyloxyphenyl)octadecan-3-one

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.10.058