ethyl 2-<3-hydroxy-2-methoxy-9-oxo-4-xanthenyloxy>-3-(4-hydroxy-3-methoxyphenyl)-3-oxopropionate

Base Information

Chemical Name:ethyl 2-<3-hydroxy-2-methoxy-9-oxo-4-xanthenyloxy>-3-(4-hydroxy-3-methoxyphenyl)-3-oxopropionate
CAS No.:126365-61-5
Molecular Formula:C₂₆H₂₂O₁₀
Molecular Weight:494.455
Hs Code.:

Synonyms:ethyl 2-<3-hydroxy-2-methoxy-9-oxo-4-xanthenyloxy>-3-(4-hydroxy-3-methoxyphenyl)-3-oxopropionate

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Chemical Property of ethyl 2-<3-hydroxy-2-methoxy-9-oxo-4-xanthenyloxy>-3-(4-hydroxy-3-methoxyphenyl)-3-oxopropionate

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Technology Process of ethyl 2-<3-hydroxy-2-methoxy-9-oxo-4-xanthenyloxy>-3-(4-hydroxy-3-methoxyphenyl)-3-oxopropionate

There total 6 articles about ethyl 2-<3-hydroxy-2-methoxy-9-oxo-4-xanthenyloxy>-3-(4-hydroxy-3-methoxyphenyl)-3-oxopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 110597-48-3
ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate

: 126365-61-5
ethyl 2-<3-hydroxy-2-methoxy-9-oxo-4-xanthenyloxy>-3-(4-hydroxy-3-methoxyphenyl)-3-oxopropionate

Guidance literature:: With hydrogen; palladium; In methanol; for 3h; Ambient temperature;

Reference yield:

: 33018-29-0
4-formyl-3-hydroxy-2-methoxyxanthone

: 126365-61-5
ethyl 2-<3-hydroxy-2-methoxy-9-oxo-4-xanthenyloxy>-3-(4-hydroxy-3-methoxyphenyl)-3-oxopropionate

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / K₂CO₃ / dimethylformamide / 1 h / 140 °C

2: m-chloroperbenzoic acid / CH₂Cl₂ / 6 h / Heating

3: 10percent KOH / methanol; CHCl₃ / Heating

4: 74 percent / t-BuOK / acetonitrile / 0.83 h / Ambient temperature

5: 89 percent / hydrogen / 5percent Pd / methanol / 3 h / Ambient temperature

With potassium hydroxide; potassium tert-butylate; hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; palladium; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 7572-90-9
ethyl 2-bromo-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

: 126365-61-5
ethyl 2-<3-hydroxy-2-methoxy-9-oxo-4-xanthenyloxy>-3-(4-hydroxy-3-methoxyphenyl)-3-oxopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / t-BuOK / acetonitrile / 0.83 h / Ambient temperature

2: 89 percent / hydrogen / 5percent Pd / methanol / 3 h / Ambient temperature

With potassium tert-butylate; hydrogen; palladium; In methanol; acetonitrile;