1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1H-pyrrole-3-carboxylic acid methyl ester

Base Information

Chemical Name:1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1H-pyrrole-3-carboxylic acid methyl ester
CAS No.:868670-30-8
Molecular Formula:C₂₂H₃₀N₂O₄
Molecular Weight:386.491
Hs Code.:

1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1<i>H</i>-pyrrole-3-carboxylic acid methyl ester

Synonyms:1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1H-pyrrole-3-carboxylic acid methyl ester

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Chemical Property of 1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1H-pyrrole-3-carboxylic acid methyl ester

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Technology Process of 1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1H-pyrrole-3-carboxylic acid methyl ester

There total 5 articles about 1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1H-pyrrole-3-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 400652-46-2,346669-50-9
((S)-2-amino-1-methyl-ethyl)-carbamic acid benzyl ester

: 665006-14-4
5-(methoxycarbonyl)-3,6-nonanedione

: 868670-30-8
1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1H-pyrrole-3-carboxylic acid methyl ester

Guidance literature:: With acetic acid; at 130 ℃; under 10343 Torr; microwave assisted;
DOI:10.1016/j.tetlet.2005.07.155

Reference yield:

: 3-hydroxy-2-(2-oxo-butyl)-hexanoic acid methyl ester

: 868670-30-8
1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1H-pyrrole-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PCC / CH₂Cl₂ / 12 h / 20 °C

2: 65 percent / AcOH / 130 °C / 10343 Torr / microwave assisted

With acetic acid; pyridinium chlorochromate; In dichloromethane; 2: Paal-Knorr reaction;
DOI:10.1016/j.tetlet.2005.07.155

Reference yield:

: 30414-53-0
methyl propanoyl acetate

: 868670-30-8
1-(2-benzyloxycarbonylamino-propyl)-5-ethyl-2-propyl-1H-pyrrole-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₂Zn / CH₂Cl₂ / 2 h / 20 °C

2: PCC / CH₂Cl₂ / 12 h / 20 °C

3: 65 percent / AcOH / 130 °C / 10343 Torr / microwave assisted

With diethylzinc; acetic acid; pyridinium chlorochromate; In dichloromethane; 3: Paal-Knorr reaction;
DOI:10.1016/j.tetlet.2005.07.155