N-(tert-butyldimethylsilyloxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene

Base Information

Chemical Name:N-(tert-butyldimethylsilyloxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene
CAS No.:114671-07-7
Molecular Formula:C₁₉H₃₀ClNO₃Si
Molecular Weight:383.991
Hs Code.:

Synonyms:N-(tert-butyldimethylsilyloxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene

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Chemical Property of N-(tert-butyldimethylsilyloxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene

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Technology Process of N-(tert-butyldimethylsilyloxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene

There total 5 articles about N-(tert-butyldimethylsilyloxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 124754-55-8
(2R)-N-(tert-butoxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene

: 114671-07-7
N-(tert-butyldimethylsilyloxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; for 0.25h; Ambient temperature;

Reference yield:

: 92085-86-4
(+)-tert-butyl {(1R)-1-[(benzyloxy)methyl]prop-2-en-1-yl}carbamate

: 114671-07-7
N-(tert-butyldimethylsilyloxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) O₃, 2.) (CH₃)2S / 1.) MeOH, -78 deg C, 2a.) -78 deg C, b.) RT, 18 h

2: 57 percent / benzene / 2 h / 40 °C

3: 67 percent / lithium tri-tert-butoxyaluminohydride / tetrahydrofuran / 2 h / -78 - -30 °C

4: 85 percent / Ph₃P, N-chlorosuccinimide / CH₂Cl₂ / 1 h / 0 °C

5: 2,6-lutidine / CH₂Cl₂ / 0.25 h / Ambient temperature

With 2,6-dimethylpyridine; N-chloro-succinimide; lithium tri(t-butoxy)aluminum hydride; dimethylsulfide; ozone; triphenylphosphine; In tetrahydrofuran; dichloromethane; benzene;

Reference yield:

: 124754-86-5
((E)-(R)-1-Benzyloxymethyl-4-oxo-but-2-enyl)-carbamic acid tert-butyl ester

: 114671-07-7
N-(tert-butyldimethylsilyloxycarbonyl)-2-amino-1-(benzyloxy)-5-chloro-3-pentene

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / lithium tri-tert-butoxyaluminohydride / tetrahydrofuran / 2 h / -78 - -30 °C

2: 85 percent / Ph₃P, N-chlorosuccinimide / CH₂Cl₂ / 1 h / 0 °C

3: 2,6-lutidine / CH₂Cl₂ / 0.25 h / Ambient temperature

With 2,6-dimethylpyridine; N-chloro-succinimide; lithium tri(t-butoxy)aluminum hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane;