2-hydroxy-4-(β-D-tetra-O-acetylglucopyranosyloxy)phenyl 4-methoxybenzyl ketone

Base Information

Chemical Name:2-hydroxy-4-(β-D-tetra-O-acetylglucopyranosyloxy)phenyl 4-methoxybenzyl ketone
CAS No.:42868-73-5
Molecular Formula:C₂₉H₃₂O₁₃
Molecular Weight:588.565
Hs Code.:

Synonyms:2-hydroxy-4-(β-D-tetra-O-acetylglucopyranosyloxy)phenyl 4-methoxybenzyl ketone

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Chemical Property of 2-hydroxy-4-(β-D-tetra-O-acetylglucopyranosyloxy)phenyl 4-methoxybenzyl ketone

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Technology Process of 2-hydroxy-4-(β-D-tetra-O-acetylglucopyranosyloxy)phenyl 4-methoxybenzyl ketone

There total 4 articles about 2-hydroxy-4-(β-D-tetra-O-acetylglucopyranosyloxy)phenyl 4-methoxybenzyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 487-49-0
1-(2,4-dihydroxyphenyl)-2-(4-methoxyphenyl)ethanone

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 42868-73-5
2-hydroxy-4-(β-D-tetra-O-acetylglucopyranosyloxy)phenyl 4-methoxybenzyl ketone

Guidance literature:: With potassium hydroxide; In acetone; for 4h; Ambient temperature;
DOI:10.1007/BF00598526

Reference yield:

: 104-47-2
p-methoxybenzylnitrile

: 42868-73-5
2-hydroxy-4-(β-D-tetra-O-acetylglucopyranosyloxy)phenyl 4-methoxybenzyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: conditions of the Hoesh reaction

2: 54 percent / 50percent aq. KOH / acetone / 4 h / Ambient temperature

With potassium hydroxide; In acetone;
DOI:10.1007/BF00598526

Reference yield:

: 108-46-3
recorcinol

: 42868-73-5
2-hydroxy-4-(β-D-tetra-O-acetylglucopyranosyloxy)phenyl 4-methoxybenzyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: conditions of the Hoesh reaction

2: 54 percent / 50percent aq. KOH / acetone / 4 h / Ambient temperature

With potassium hydroxide; In acetone;
DOI:10.1007/BF00598526