N-p-tolylsulfonyl-1,5-bis(p-tolylsulfonyloxy)-3-aza-1,1,2,2,4,4,5,5-octadeuteriopentane

Base Information

Chemical Name:N-p-tolylsulfonyl-1,5-bis(p-tolylsulfonyloxy)-3-aza-1,1,2,2,4,4,5,5-octadeuteriopentane
CAS No.:1027565-28-1
Molecular Formula:C₂₅H₂₉NO₈S₃
Molecular Weight:575.642
Hs Code.:

Synonyms:N-p-tolylsulfonyl-1,5-bis(p-tolylsulfonyloxy)-3-aza-1,1,2,2,4,4,5,5-octadeuteriopentane

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Chemical Property of N-p-tolylsulfonyl-1,5-bis(p-tolylsulfonyloxy)-3-aza-1,1,2,2,4,4,5,5-octadeuteriopentane

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Technology Process of N-p-tolylsulfonyl-1,5-bis(p-tolylsulfonyloxy)-3-aza-1,1,2,2,4,4,5,5-octadeuteriopentane

There total 3 articles about N-p-tolylsulfonyl-1,5-bis(p-tolylsulfonyloxy)-3-aza-1,1,2,2,4,4,5,5-octadeuteriopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 98-59-9
p-toluenesulfonyl chloride

: N-p-tolylsulfonyl-1,1,2,2,4,4,5,5-octadeuterio-3-azapentane-1,5-diol

: 1027565-28-1
N-p-tolylsulfonyl-1,5-bis(p-tolylsulfonyloxy)-3-aza-1,1,2,2,4,4,5,5-octadeuteriopentane

Guidance literature:: In pyridine; at -18 ℃; for 336h;

Reference yield:

: 59724-90-2
(toluene-4-sulfonylimino)-di-acetic acid dimethyl ester

: 1027565-28-1
N-p-tolylsulfonyl-1,5-bis(p-tolylsulfonyloxy)-3-aza-1,1,2,2,4,4,5,5-octadeuteriopentane

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / Na / 2 h / Heating

2: 82 percent / LiAlD₄ / tetrahydrofuran / 2 h / Heating

3: 82 percent / pyridine / 336 h / -18 °C

With lithium aluminium deuteride; sodium; In tetrahydrofuran; pyridine;

Reference yield:

: bis(trideuteriomethyl) N-p-tolylsulfonyl-5-aza-2,2,4,4-tetradeuteriopentane-1,5-dioate

: 1027565-28-1
N-p-tolylsulfonyl-1,5-bis(p-tolylsulfonyloxy)-3-aza-1,1,2,2,4,4,5,5-octadeuteriopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / LiAlD₄ / tetrahydrofuran / 2 h / Heating

2: 82 percent / pyridine / 336 h / -18 °C

With lithium aluminium deuteride; In tetrahydrofuran; pyridine;