Technology Process of C10H11FO5S
There total 1 articles about C10H11FO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogensulfite;
In
ethanol; water;
at 165 ℃;
for 0.5h;
microwave reactor;
- Guidance literature:
-
With
thionyl chloride;
for 3h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 11 steps
1.1: thionyl chloride / 3 h / Reflux
2.1: triethylamine / dichloromethane / 3 h / 0 - 25 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
4.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
4.2: 8 h / -78 - 25 °C
5.1: ozone / dichloromethane / -78 °C
5.2: -78 - 25 °C
6.1: hydrogen / palladium on activated charcoal / ethanol / 760.05 Torr
7.1: diethoxyltriphenylphosphorane / toluene / 60 h / 45 °C
8.1: water; lithium hydroxide / tetrahydrofuran / 25 - 60 °C
8.2: pH 3
9.1: triethylamine; diphenyl phosphoryl azide / tetrahydrofuran / 24 h / 25 °C
9.2: 1.5 h / 80 °C
10.1: trifluoroacetic acid / 1,3-Dimethoxybenzene; chloroform / 18 h
11.1: 4 h / Reflux
11.2: 12 h / 25 °C
With
thionyl chloride; diphenyl phosphoryl azide; diethoxyltriphenylphosphorane; water; hydrogen; ozone; triethylamine; trifluoroacetic acid; lithium hydroxide; lithium diisopropyl amide;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; toluene; 1,3-Dimethoxybenzene;
