C₃₇H₄₅N₃O₇

Base Information

• Chemical Name: C₃₇H₄₅N₃O₇
• CAS No.: 1067650-21-8
• Molecular Formula: C₃₇H₄₅N₃O₇
• Molecular Weight: 643.78
• Mol file: 1067650-21-8.mol

Synonyms:C₃₇H₄₅N₃O₇

Chemical Property of C₃₇H₄₅N₃O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₄₅N₃O₇

There total 1 articles about C₃₇H₄₅N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C41H53N3O7 (935674-16-1) + di-tert-butyl dicarbonate (24424-99-5) → C37H45N3O7 (1067650-21-8)

Guidance literature:

C₄₁H₅₃N₃O₇; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;

di-tert-butyl dicarbonate; With N-ethyl-N,N-diisopropylamine; for 16h;

DOI:10.1055/s-2008-1067171

Reference yield: 56.0%

C37H45N3O7 (1067650-21-8) + acetic anhydride (108-24-7) → Ac-[Lys-βNspe]5-NH2 (1030834-37-7)

Guidance literature:

C₃₇H₄₅N₃O₇; With polyethylene glycol polyamide resin; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h; Automated synthesizer; solid phase reaction;

With piperidine; In N,N-dimethyl-formamide; Automated synthesizer; solid phase reaction;

C₃₇H₄₅N₃O₇; acetic anhydride; Further stages;

DOI:10.1055/s-2008-1067171

Reference yield: 47.0%

C37H45N3O7 (1067650-21-8) + acetic anhydride (108-24-7) → Ac-[Lys-βNspe]6-NH2

Guidance literature:

C₃₇H₄₅N₃O₇; With polyethylene glycol polyamide resin; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h; Automated synthesizer; solid phase reaction;

With piperidine; In N,N-dimethyl-formamide; Automated synthesizer; solid phase reaction;

C₃₇H₄₅N₃O₇; acetic anhydride; Further stages;

DOI:10.1055/s-2008-1067171

upstream raw materials:

C₄₁H₅₃N₃O₇

di-tert-butyl dicarbonate

Downstream raw materials:

Ac-[Lys-βNspe]5-NH2

Ac-[Lys-βNspe]7-NH2

C₁₃₈H₂₀₅N₂₅O₁₇