1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside

Base Information

• Chemical Name: 1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside
• CAS No.: 1206803-50-0
• Molecular Formula: C₆₆H₈₆O₁₁Si₂
• Molecular Weight: 1111.57

Synonyms:1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside

Chemical Property of 1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of 1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside

There total 2 articles about 1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

triethylsilane (617-86-7) + 1,3,4,6-tetra-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (18685-22-8) → 1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside (1206803-50-0)

Guidance literature:

triethylsilane; With dicobalt octacarbonyl; carbon monoxide; at 20 ℃; for 0.333333h;

1,3,4,6-tetra-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside; In toluene; regioselective reaction; Reflux;

DOI:10.1016/j.tet.2013.03.094

Reference yield: 85.0%

triethylsilane (617-86-7) + 1,3,4,6-tetra-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (18685-22-8) → 1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside (1206803-49-7) + 1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside (1206803-50-0)

Guidance literature:

triethylsilane; With dicobalt octacarbonyl; carbon monoxide; at 20 ℃; for 0.333333h;

1,3,4,6-tetra-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside; In benzene; at 50 ℃; regioselective reaction;

DOI:10.1016/j.tet.2013.03.094

Reference yield:

1,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-fructofuranosyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-α-D-glucopyranoside (1206803-50-0) → 1’,2,3,3’,4,4’-hexa-O-benzylsucrose (74761-34-5)

Guidance literature:

With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/ol902717y

upstream raw materials:

triethylsilane

1,3,4,6-tetra-O-benzyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Downstream raw materials:

1’,2,3,3’,4,4’-hexa-O-benzylsucrose

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