Technology Process of C26H39NO8
There total 6 articles about C26H39NO8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
10 wt% Pd(OH)2 on carbon; hydrogen;
In
methanol;
at 25 ℃;
for 1h;
under 760.051 Torr;
DOI:10.1021/ja203754p
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / dichloromethane; water / 4 h / 20 °C
2.1: (2R)-(+)-3,3'-diphenyl-[2,2'-dinaphthalene]-1,1'-diol; C38H25BO3; C44H30B2O5 / dichloromethane / 10 h / -78 °C / Inert atmosphere
3.1: methylmagnesium bromide / Inert atmosphere
3.2: 0.05 h / 0 °C / Inert atmosphere
4.1: 10 wt% Pd(OH)2 on carbon; hydrogen / methanol / 1 h / 25 °C / 760.05 Torr
With
(2R)-(+)-3,3'-diphenyl-[2,2'-dinaphthalene]-1,1'-diol; C38H25BO3; C44H30B2O5; 10 wt% Pd(OH)2 on carbon; methylmagnesium bromide; hydrogen; potassium carbonate;
In
methanol; dichloromethane; water;
DOI:10.1021/ja203754p
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methylmagnesium bromide / Inert atmosphere
1.2: 0.05 h / 0 °C / Inert atmosphere
2.1: 10 wt% Pd(OH)2 on carbon; hydrogen / methanol / 1 h / 25 °C / 760.05 Torr
With
10 wt% Pd(OH)2 on carbon; methylmagnesium bromide; hydrogen;
In
methanol;
DOI:10.1021/ja203754p