Technology Process of C20H24O3
There total 3 articles about C20H24O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
methanol;
DOI:10.1021/ol300434m
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tert.-butyl lithium / pentane; diethyl ether / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.5 h / 0 - 20 °C
With
sodium tetrahydroborate; cerium(III) chloride heptahydrate; tert.-butyl lithium;
In
methanol; diethyl ether; pentane;
DOI:10.1021/jo5023266
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tert.-butyl lithium / pentane; diethyl ether / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.5 h / 0 - 20 °C
With
sodium tetrahydroborate; cerium(III) chloride heptahydrate; tert.-butyl lithium;
In
methanol; diethyl ether; pentane;
DOI:10.1021/jo5023266