1-(p-bromophenyl)-2-nitroethylcarbamic acid t-butyl ester

Base Information

Chemical Name:1-(p-bromophenyl)-2-nitroethylcarbamic acid t-butyl ester
CAS No.:1140969-68-1
Molecular Formula:C₁₃H₁₇BrN₂O₄
Molecular Weight:345.193
Hs Code.:

Synonyms:1-(p-bromophenyl)-2-nitroethylcarbamic acid t-butyl ester

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Chemical Property of 1-(p-bromophenyl)-2-nitroethylcarbamic acid t-butyl ester

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Technology Process of 1-(p-bromophenyl)-2-nitroethylcarbamic acid t-butyl ester

There total 2 articles about 1-(p-bromophenyl)-2-nitroethylcarbamic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75-52-5
nitromethane

: 479423-43-3
tert-butyl 4-bromobenzylidenecarbamate

: 1140969-68-1
1-(p-bromophenyl)-2-nitroethylcarbamic acid t-butyl ester

Guidance literature:: With (S)-1-(1-Naphthyl)ethylamine; triethylamine; In toluene; at -25 - 20 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1016/j.tetasy.2011.05.006

Reference yield:

: 75-52-5
nitromethane

: 479423-43-3
tert-butyl 4-bromobenzylidenecarbamate

: 1140969-68-1
1-(p-bromophenyl)-2-nitroethylcarbamic acid t-butyl ester

: 1-(p-bromophenyl)-2-nitroethylcarbamic acid t-butyl ester

Guidance literature:: With (R)-1-(3,5-bis-trifluoromethylphenyl)-3-{2'-[3-(3,5-bis-trifluoromethylphenyl)thioureido]-[1,1']binaphthalenyl-2-yl}-thiourea; triethylamine; In toluene; at -35 ℃; for 24h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/adsc.200800214