(2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester

Base Information

Chemical Name:(2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester
CAS No.:1391748-84-7
Molecular Formula:C₄₇H₆₄N₆O₈
Molecular Weight:841.061
Hs Code.:

(2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester

Synonyms:(2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester

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Chemical Property of (2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester

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Technology Process of (2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester

There total 3 articles about (2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1391748-83-6
(2-aminoethyl)-(2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)carbamic acid tert-butyl ester

: 70700-35-5
trimethyl-[2-(4-nitrophenyl)allyl]ammonium iodide

: 1391748-84-7
(2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In methanol; at 50 ℃; for 72h; Inert atmosphere;
DOI:10.1002/anie.201200822

Reference yield:

: 642-31-9
9-anthracene aldehyde

: 1391748-84-7
(2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 72 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 24 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / methanol / 72 h / 50 °C / Inert atmosphere

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In methanol; ethanol;
DOI:10.1002/anie.201200822

Reference yield:

: C₃₈H₅₅N₅O₆

: 1391748-84-7
(2-{[2-({2-[(anthracen-9-ylmethyl)amino]ethyl}-tert-butoxycarbonylamino)ethyl]-tert-butoxycarbonylamino}ethyl)-{2-[2-(4-nitrophenyl)allylamino]ethyl}carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 24 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / methanol / 72 h / 50 °C / Inert atmosphere

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In methanol; ethanol;
DOI:10.1002/anie.201200822