C₁₉H₂₂NOP

Base Information

• Chemical Name: C₁₉H₂₂NOP
• CAS No.: 172847-62-0
• Molecular Formula: C₁₉H₂₂NOP
• Molecular Weight: 311.364
• Mol file: 172847-62-0.mol

Synonyms:C₁₉H₂₂NOP

Chemical Property of C₁₉H₂₂NOP

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₂₂NOP

There total 1 articles about C₁₉H₂₂NOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-3,4-dimethylcyclopentanone (19550-72-2) → C19H22NOP (172847-62-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / NH₂OH*HCl, NaOAc / H₂O; methanol / 60 °C

2: Et₃N / CH₂Cl₂; petroleum ether / 2 h / -50 °C

With hydroxylamine hydrochloride; sodium acetate; triethylamine; In methanol; dichloromethane; water; Petroleum ether;

DOI:10.1021/jo00128a009

Reference yield: 66.0%

C19H22NOP (172847-62-0) → N-(Diphenylphosphinyl)-cis-3,4-dimethylcyclopentylamine

Guidance literature:

With L-Selectride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1021/jo00128a009

Reference yield:

C19H22NOP (172847-62-0) → N-(Diphenylphosphinyl)-cis-3,4-dimethylcyclopentylamine + N-(Diphenylphosphinyl)-cis-3,4-dimethylcyclopentylamine

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1021/jo00128a009

upstream raw materials:

cis-3,4-dimethylcyclopentanone