phenylethylny-(2,6-bis(pyridin-2-yl)pyridine)-platinum(II) hexafluorophosphate

Base Information

Chemical Name:phenylethylny-(2,6-bis(pyridin-2-yl)pyridine)-platinum(II) hexafluorophosphate
CAS No.:376362-92-4
Molecular Formula:C₂₃H₁₆N₃Pt*F₆P
Molecular Weight:674.444
Hs Code.:

Synonyms:phenylethylny-(2,6-bis(pyridin-2-yl)pyridine)-platinum(II) hexafluorophosphate

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Chemical Property of phenylethylny-(2,6-bis(pyridin-2-yl)pyridine)-platinum(II) hexafluorophosphate

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Technology Process of phenylethylny-(2,6-bis(pyridin-2-yl)pyridine)-platinum(II) hexafluorophosphate

There total 4 articles about phenylethylny-(2,6-bis(pyridin-2-yl)pyridine)-platinum(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 166268-06-0
chloro(2,2’:6’,2’’-terpyridine)platinum(II) hexafluorophosphate

: 536-74-3
phenylacetylene

: 376362-92-4
phenylethylny-(2,6-bis(pyridin-2-yl)pyridine)-platinum(II) hexafluorophosphate

Guidance literature:: With copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 55 ℃; for 48h; Sealed tube; Inert atmosphere; Darkness;
DOI:10.1002/cctc.201800345

Reference yield: 60.0%

: ammonium hexafluorophosphate

: [Pt(2,2′:6′,2″-terpyridine)(MeCN)](OTf)₂

: 536-74-3
phenylacetylene

: 376362-92-4
phenylethylny-(2,6-bis(pyridin-2-yl)pyridine)-platinum(II) hexafluorophosphate

Guidance literature:: With NaOH; In methanol; NaOH was added to stirred soln. of phenylacetylene in methanol; soln. was stirred at room temp. for 30 min; Pt complex was added; mixt. was stirred at room temp. for 12 h; filtered; satd. soln. of NH4PF6 in methanol was added to filtrate; filtered; washed (methanol); dried; recrystn. by diffusion of Et2O vaporinto a CH3CN soln.; elem. anal.;
DOI:10.1021/om010336x

Reference yield: 37.1%

: ammonium hexafluorophosphate

: 60819-00-3
chloro(2,2':6',2''-terpyridine)platinum(II) chloride

: 536-74-3
phenylacetylene

: 376362-92-4
phenylethylny-(2,6-bis(pyridin-2-yl)pyridine)-platinum(II) hexafluorophosphate

Guidance literature:: chloro(2,2':6',2''-terpyridine)platinum(II) chloride; phenylacetylene; With copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 72h; Inert atmosphere;

ammonium hexafluorophosphate; In water; N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.3390/molecules24030404