1-(4-chloro-phenyl)-5-(4-chloro-phenylazo)-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid methyl ester

Base Information

• Chemical Name: 1-(4-chloro-phenyl)-5-(4-chloro-phenylazo)-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid methyl ester
• CAS No.: 82522-94-9
• Molecular Formula: C₁₈H₁₂Cl₂N₄O₃
• Molecular Weight: 403.224

Synonyms:1-(4-chloro-phenyl)-5-(4-chloro-phenylazo)-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid methyl ester

Chemical Property of 1-(4-chloro-phenyl)-5-(4-chloro-phenylazo)-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-(4-chloro-phenyl)-5-(4-chloro-phenylazo)-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid methyl ester

There total 2 articles about 1-(4-chloro-phenyl)-5-(4-chloro-phenylazo)-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl glutaconate (5164-76-1) → 1-(4-chloro-phenyl)-5-(4-chloro-phenylazo)-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid methyl ester (82522-94-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium acetate; aqueous methanol

2: methanol

With methanol; sodium acetate;

DOI:10.1021/ja01599a042

Reference yield:

2-(4-chloro-phenylazo)-4-(4-chloro-phenylhydrazono)-pentenedioic acid dimethyl ester (82522-87-0) → 1-(4-chloro-phenyl)-5-(4-chloro-phenylazo)-6-oxo-1,6-dihydro-pyridazine-3-carboxylic acid methyl ester (82522-94-9)

Guidance literature:

With methanol;

DOI:10.1021/ja01599a042

upstream raw materials:

2-(4-chloro-phenylazo)-4-(4-chloro-phenylhydrazono)-pentenedioic acid dimethyl ester

dimethyl glutaconate

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