4-(2-cyclohexyl-1,1-dimethylethylperoxy)-5-ethoxycarbonyl-2-phenylpyrimidin

Base Information

Chemical Name:4-(2-cyclohexyl-1,1-dimethylethylperoxy)-5-ethoxycarbonyl-2-phenylpyrimidin
CAS No.:135370-80-8
Molecular Formula:C₂₃H₃₀N₂O₄
Molecular Weight:398.502
Hs Code.:

Synonyms:4-(2-cyclohexyl-1,1-dimethylethylperoxy)-5-ethoxycarbonyl-2-phenylpyrimidin

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Chemical Property of 4-(2-cyclohexyl-1,1-dimethylethylperoxy)-5-ethoxycarbonyl-2-phenylpyrimidin

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Technology Process of 4-(2-cyclohexyl-1,1-dimethylethylperoxy)-5-ethoxycarbonyl-2-phenylpyrimidin

There total 2 articles about 4-(2-cyclohexyl-1,1-dimethylethylperoxy)-5-ethoxycarbonyl-2-phenylpyrimidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 135370-74-0
2-cyclohexyl-1,1-dimethylethylhydroperoxid

: 24755-82-6
ethyl 4-chloro-2-phenylpyrimidine-5-carboxylate

: 135370-80-8
4-(2-cyclohexyl-1,1-dimethylethylperoxy)-5-ethoxycarbonyl-2-phenylpyrimidin

Guidance literature:: With barium(II) oxide; In Petroleum ether; at 0 ℃; for 24h;

Reference yield:

: 5531-30-6
2-cyclohexyl-1,1-dimethyl ethanol

: 135370-80-8
4-(2-cyclohexyl-1,1-dimethylethylperoxy)-5-ethoxycarbonyl-2-phenylpyrimidin

Guidance literature:: Multi-step reaction with 2 steps

1: 87.5 percent / 50percent aq. H₂O₂, 85percent aq. phosphoric acid / 6 h / 50 °C

2: 50 percent / BaO / petroleum ether / 24 h / 0 °C

With phosphoric acid; dihydrogen peroxide; barium(II) oxide; In Petroleum ether;