17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trien-8R-ol

Base Information

• Chemical Name: 17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trien-8R-ol
• CAS No.: 1234501-61-1
• Molecular Formula: C₃₆H₆₁IO₄Si
• Molecular Weight: 712.868

Synonyms:17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trien-8R-ol

Chemical Property of 17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trien-8R-ol

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Technology Process of 17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trien-8R-ol

There total 1 articles about 17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trien-8R-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trienone (1234502-04-5) → 17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trien-8S-ol + 17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trien-8R-ol (1234501-61-1)

Guidance literature:

17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trienone; With lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; at 0 ℃; for 24h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water; optical yield given as %de; Inert atmosphere;

DOI:10.1021/ja103537u

Reference yield: 99.0%

17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trien-8R-ol (1234501-61-1) + triethylsilyl trifluoromethyl sulfonate (79271-56-0) → 1S-[12-iodo-2S,6S,8S,10S-tetramethyl-1S-(1-methylpenta-2Z,4-dienyl)-3R,9R-bis(triethylsilanyloxy)dodec-11Z-enyloxymethyl]-4-methoxybenzene (1234502-05-6)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;

DOI:10.1021/ja103537u

upstream raw materials:

17-iodo-6S-(4-methoxybenzyloxy)-5S,7S,11S,13S,15S-pentamethyl-14R-(triethylsilanyloxy)heptadeca-1,3Z,16Z-trienone

Downstream raw materials:

1S-[12-iodo-2S,6S,8S,10S-tetramethyl-1S-(1-methylpenta-2Z,4-dienyl)-3R,9R-bis(triethylsilanyloxy)dodec-11Z-enyloxymethyl]-4-methoxybenzene

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