t-Butyl 3-Oxo-2-(α-(2-methoxyethoxy)methoxy-4-fluorobenzyl)-1-piperazine carboxylate

Base Information

Chemical Name:t-Butyl 3-Oxo-2-(α-(2-methoxyethoxy)methoxy-4-fluorobenzyl)-1-piperazine carboxylate
CAS No.:78665-16-4
Molecular Formula:C₂₀H₂₉FN₂O₆
Molecular Weight:412.458
Hs Code.:

Synonyms:t-Butyl 3-Oxo-2-(α-(2-methoxyethoxy)methoxy-4-fluorobenzyl)-1-piperazine carboxylate

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Chemical Property of t-Butyl 3-Oxo-2-(α-(2-methoxyethoxy)methoxy-4-fluorobenzyl)-1-piperazine carboxylate

Chemical Property:

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Technology Process of t-Butyl 3-Oxo-2-(α-(2-methoxyethoxy)methoxy-4-fluorobenzyl)-1-piperazine carboxylate

There total 2 articles about t-Butyl 3-Oxo-2-(α-(2-methoxyethoxy)methoxy-4-fluorobenzyl)-1-piperazine carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78665-15-3
t-Butyl 3-Oxo-2-(α-hydroxy-4-fluorobenzyl)-1-piperazine carboxylate

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 78665-16-4
t-Butyl 3-Oxo-2-(α-(2-methoxyethoxy)methoxy-4-fluorobenzyl)-1-piperazine carboxylate

Guidance literature:: With NaH; In N-methyl-acetamide; water; N,N-dimethyl-formamide;

Reference yield:

: 889958-14-9
tert-butyl 2-oxopiperazine-1-carboxylate

: 459-57-4
4-fluorobenzaldehyde

: 78665-16-4
t-Butyl 3-Oxo-2-(α-(2-methoxyethoxy)methoxy-4-fluorobenzyl)-1-piperazine carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane

2: NaH / N-methyl-acetamide; water; N,N-dimethyl-formamide

With n-butyllithium; NaH; diisopropylamine; In tetrahydrofuran; N-methyl-acetamide; hexane; water; N,N-dimethyl-formamide;