N-ethyl-N-<6-<(3,4-dimethoxybenzoyl)oxy>hexyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

Base Information

• Chemical Name: N-ethyl-N-<6-<(3,4-dimethoxybenzoyl)oxy>hexyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine
• CAS No.: 69788-32-5
• Molecular Formula: C₂₈H₃₉NO₅
• Molecular Weight: 469.621

Synonyms:N-ethyl-N-<6-<(3,4-dimethoxybenzoyl)oxy>hexyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

Chemical Property of N-ethyl-N-<6-<(3,4-dimethoxybenzoyl)oxy>hexyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

Chemical Property:

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Technology Process of N-ethyl-N-<6-<(3,4-dimethoxybenzoyl)oxy>hexyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

There total 3 articles about N-ethyl-N-<6-<(3,4-dimethoxybenzoyl)oxy>hexyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-methoxy-2-tetralone (2472-22-2) → N-ethyl-N-<6-<(3,4-dimethoxybenzoyl)oxy>hexyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine (69788-32-5)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / PtO₂ / ethanol

2: Na₂CO₃ / butan-2-one / 40 h / Heating

With hydrogen; sodium carbonate; platinum(IV) oxide; In ethanol; butanone;

DOI:10.1021/jm00353a016

Reference yield:

N-ethyl-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine (69788-93-8) + 6-iodohexyl 3,4-dimethoxybenzoate → N-ethyl-N-<6-<(3,4-dimethoxybenzoyl)oxy>hexyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine (69788-32-5)

Guidance literature:

With sodium carbonate; In butanone; for 40h; Heating;

DOI:10.1021/jm00353a016

Reference yield:

6-chlorohexyl-3,4-dimethoxybenzoate (69788-73-4) + N-ethyl-6-methoxy-1,2,3,4-tetrahydro-2-naphthylamine hydrochloride (69788-71-2) → N-ethyl-N-<6-<(3,4-dimethoxybenzoyl)oxy>hexyl>-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine (69788-32-5)

Guidance literature:

Multistep reaction; (i) aq. NaOH, (ii) /BRN= 5047177/, NaI, Na₂CO₃, MeCOEt;

upstream raw materials:

6-chlorohexyl-3,4-dimethoxybenzoate

N-ethyl-6-methoxy-1,2,3,4-tetrahydro-2-naphthylamine hydrochloride

N-ethyl-1,2,3,4-tetrahydro-6-methoxy-2-naphthylamine

6-methoxy-2-tetralone

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