Technology Process of C31H43NOSi
There total 3 articles about C31H43NOSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
C22H36P2; cobalt(II) diacetate tetrahydrate; zinc;
In
tert-Amyl alcohol; dimethyl sulfoxide;
at 80 ℃;
for 20h;
enantioselective reaction;
DOI:10.1021/ja309756k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 24 h / 0 - 20 °C
2: pyridine / dichloromethane / 24 h / 0 - 20 °C
3: C22H36P2; cobalt(II) diacetate tetrahydrate; zinc / dimethyl sulfoxide; tert-Amyl alcohol / 20 h / 80 °C
With
pyridine; oxalyl dichloride; C22H36P2; cobalt(II) diacetate tetrahydrate; N,N-dimethyl-formamide; zinc;
In
tert-Amyl alcohol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja309756k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / dichloromethane / 24 h / 0 - 20 °C
2: C22H36P2; cobalt(II) diacetate tetrahydrate; zinc / dimethyl sulfoxide; tert-Amyl alcohol / 20 h / 80 °C
With
pyridine; C22H36P2; cobalt(II) diacetate tetrahydrate; zinc;
In
tert-Amyl alcohol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja309756k