{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}⁽²⁺⁾*2I^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}I₂

Base Information

• Chemical Name: {(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}⁽²⁺⁾*2I^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}I₂
• CAS No.: 110391-67-8
• Molecular Formula: C₄₈H₅₄ClP₄RhS₂*2I
• Molecular Weight: 1211.15

Synonyms:{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}⁽²⁺⁾*2I^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}I₂

Chemical Property of {(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}⁽²⁺⁾*2I^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}I₂

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Technology Process of {(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}⁽²⁺⁾*2I^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}I₂

There total 1 articles about {(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}⁽²⁺⁾*2I^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}I₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

{(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)} (100044-10-8) → {(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)}(2+)*2I(1-)={(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)}I2 (110391-67-8)

Guidance literature:

With I₂; In tetrahydrofuran; dropwise addn. of a THF soln. of I2 to a stirred soln. of (triphos)RhCl(S2CP(Et)3) in THF under N2 atm.; mechanism discussed;; ppt.; dried in a stream of N2; elem. anal.;;

Reference yield:

{(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)}(2+)*2I(1-)={(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)}I2 (110391-67-8) → {(CH3C(CH2P(C6H5)2)3)RhCl(S2CO)} (100044-11-9)

Guidance literature:

Multi-step reaction with 4 steps

1: I₂ / tetrahydrofuran

2: ethanol / ethanol; N,N-dimethyl-formamide

3: ethanol; dichloromethane

4: O₂ / dichloromethane; N,N-dimethyl-formamide

With I₂; ethanol; O₂; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

{(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)}(2+)*2I(1-)={(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)}I2 (110391-67-8) → {(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)}(2+)*2I3(1-)={(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)}(I3)2 (110416-97-2)

Guidance literature:

With I₂; In tetrahydrofuran; treatment of a suspension of ((triphos)RhCl(S2CPEt3))I2 in THF with a 3-fold excess of I2 in N2 atm.;; dried in a stream of N2; elem. anal.;;

upstream raw materials:

{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}

Downstream raw materials:

{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}⁽²⁺⁾*2I₃^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}(I₃)2

{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}⁽¹⁺⁾*I₃^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}(I₃)

{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}⁽¹⁺⁾*B(C₆H₅)4^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}B(C₆H₅)4

{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CO)}

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