3-(2-[4-[maleimid-1-yl]phenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone

Base Information

Chemical Name:3-(2-[4-[maleimid-1-yl]phenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone
CAS No.:281674-30-4
Molecular Formula:C₂₃H₁₉N₃O₅
Molecular Weight:417.421
Hs Code.:

Synonyms:3-(2-[4-[maleimid-1-yl]phenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone

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Chemical Property of 3-(2-[4-[maleimid-1-yl]phenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone

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Technology Process of 3-(2-[4-[maleimid-1-yl]phenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone

There total 5 articles about 3-(2-[4-[maleimid-1-yl]phenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 3-(2-[4-[3-hydroxycarbonyl]propenamidophenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone

: 281674-30-4
3-(2-[4-[maleimid-1-yl]phenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone

Guidance literature:: With sodium acetate; acetic anhydride; for 24h; Heating;

Reference yield:

: 122-85-0
para-acetamidobenzaldehyde

: 281674-30-4
3-(2-[4-[maleimid-1-yl]phenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone

Guidance literature:: Multi-step reaction with 4 steps

1: 42 percent / piperidine; glacial AcOH / methanol / 24 h / Heating

2: 79 percent / aq. KOH / methanol / 24 h / Heating

3: 97 percent / CHCl₃ / 24 h / Heating

4: 47 percent / NaOAc; Ac₂O / 24 h / Heating

With piperidine; potassium hydroxide; sodium acetate; acetic anhydride; acetic acid; In methanol; chloroform; 1: Condensation / 2: Deacetylation / 3: Condensation / 4: Cyclization;

Reference yield:

: 5761-60-4
6,7-dimethoxy-1,3-dimethyl-2(1H)-oxoquinoxaline

: 281674-30-4
3-(2-[4-[maleimid-1-yl]phenyl]ethenyl)-6,7-dimethoxy-1-methyl-2(1H)-quinoxalinone

Guidance literature:: Multi-step reaction with 4 steps

1: 42 percent / piperidine; glacial AcOH / methanol / 24 h / Heating

2: 79 percent / aq. KOH / methanol / 24 h / Heating

3: 97 percent / CHCl₃ / 24 h / Heating

4: 47 percent / NaOAc; Ac₂O / 24 h / Heating

With piperidine; potassium hydroxide; sodium acetate; acetic anhydride; acetic acid; In methanol; chloroform; 1: Condensation / 2: Deacetylation / 3: Condensation / 4: Cyclization;