ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate

Base Information

Chemical Name:ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate
CAS No.:1450740-56-3
Molecular Formula:C₁₈H₂₂O₆
Molecular Weight:334.369
Hs Code.:

Synonyms:ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate

Suppliers and Price of ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate

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Technology Process of ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate

There total 1 articles about ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1450740-56-3
ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: morpholin-4-ium 2,2,2-trifluoroacetate / 80 °C / Sealed tube

2.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

With morpholin-4-ium 2,2,2-trifluoroacetate; lithium diisopropyl amide; In tetrahydrofuran; 1.1: |Aldol Condensation;
DOI:10.1016/j.bmc.2013.06.044

Reference yield: 50.0%

: 1450740-56-3
ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate

: 1450740-30-3
5-methyl-5-[(E)-2-(3,4,5-trimethoxyphenyl)ethenyl]-2,5-dihydrofuran-2-one

Guidance literature:: ehyl (5E)-4-hydroxy-4-methyl-6-(3,4,5-trimethoxyphenyl)hex-5-en-2-ynoate; With quinoline; hydrogen; In methanol; at 20 ℃; for 3h;

In methanol; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2013.06.044