(2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate

Base Information

Chemical Name:(2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate
CAS No.:133030-44-1
Molecular Formula:C₂₃H₂₈O₃S
Molecular Weight:384.54
Hs Code.:

Synonyms:(2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate

Suppliers and Price of (2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate

There total 1 articles about (2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51233-80-8
2,6-dimethylphenyl propionate

: 115205-40-8
1-phenylsulfanylcyclopentane carboxaldehyde

: 133030-44-1
(2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 degC, 10 min 2.) -78 degC, 5 min;

Reference yield: 90.0%

: 133030-44-1
(2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate

: 120749-37-3,133030-55-4,138751-07-2
(1RS,2RS)-2-methyl-1-<1-(phenylthio)cyclopentyl>propane-1,3-diol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 3h;
DOI:10.1039/b106851b

Reference yield:

: 133030-44-1
(2RS,3SR)-2,6-dimethylphenyl 3-hydroxy-2-methyl-3-<1-(phenylthio)cyclopentyl>propionate

: (2R*,3S*)-3-methyl-2-(1'-phenylsulfonylcyclopentyl)oxetane

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / LiAlH₄ / diethyl ether / 3 h / 20 °C

2: 79 percent / MCPBA; Na₂HPO₄ / CH₂Cl₂ / 6 h / 0 °C

3: 86 percent / DEAD; zinc N,N-dimethyldithiacarbamaye; Ph₃P / toluene / 0.08 h

With disodium hydrogenphosphate; lithium aluminium tetrahydride; Ziram; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate; In diethyl ether; dichloromethane; toluene; 3: Mitsunobu reaction;
DOI:10.1039/b106851b