C₂HF₃O₂*C₂₄H₂₃ClN₆O

Base Information

Chemical Name:C₂HF₃O₂*C₂₄H₂₃ClN₆O
CAS No.:1396673-08-7
Molecular Formula:C₂HF₃O₂*C₂₄H₂₃ClN₆O
Molecular Weight:560.963
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>24</sub>H<sub>23</sub>ClN<sub>6</sub>O

Synonyms:C₂HF₃O₂*C₂₄H₂₃ClN₆O

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Chemical Property of C₂HF₃O₂*C₂₄H₂₃ClN₆O

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Technology Process of C₂HF₃O₂*C₂₄H₂₃ClN₆O

There total 8 articles about C₂HF₃O₂*C₂₄H₂₃ClN₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1375701-71-5
(4-{4-[5-(5-chloro-1H-benzimidazol-2-yl)pyridin-2-yl]piperazin-1-yl}phenyl)acetic acid

: 1396673-08-7
C₂HF₃O₂*C₂₄H₂₃ClN₆O

Guidance literature:: (4-{4-[5-(5-chloro-1H-benzimidazol-2-yl)pyridin-2-yl]piperazin-1-yl}phenyl)acetic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; for 2h;

With ammonia; In 1,4-dioxane; N,N-dimethyl-formamide; for 16h; Sealed tube;

With trifluoroacetic acid; In water; acetonitrile;

Reference yield:

: 14062-25-0
Ethyl 4-bromophenylacetate

: 1396673-08-7
C₂HF₃O₂*C₂₄H₂₃ClN₆O

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate / palladium diacetate; XPhos / ISOPROPYLAMIDE / 1 h / 150 °C / Inert atmosphere; Microwave irradiation

2.1: hydrogen / palladium hydroxide, 20 wt% on carbon / ethanol / 16 h / 760.05 Torr

3.1: N-ethyl-N,N-diisopropylamine / ISOPROPYLAMIDE / 16 h / 110 °C

4.1: sodium hydroxide; water / tetrahydrofuran / 22 h / 20 - 50 °C

5.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 2 h

5.2: 16 h / Sealed tube

With water; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; sodium hydroxide; palladium hydroxide, 20 wt% on carbon; palladium diacetate; XPhos; In tetrahydrofuran; ethanol; ISOPROPYLAMIDE; N,N-dimethyl-formamide;

Reference yield:

: 1375702-42-3
ethyl [4-(4-benzylpiperazin-1-yl)phenyl]acetate

: 1396673-08-7
C₂HF₃O₂*C₂₄H₂₃ClN₆O

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / palladium hydroxide, 20 wt% on carbon / ethanol / 16 h / 760.05 Torr

2.1: N-ethyl-N,N-diisopropylamine / ISOPROPYLAMIDE / 16 h / 110 °C

3.1: sodium hydroxide; water / tetrahydrofuran / 22 h / 20 - 50 °C

4.1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 2 h

4.2: 16 h / Sealed tube

With water; hydrogen; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; sodium hydroxide; palladium hydroxide, 20 wt% on carbon; In tetrahydrofuran; ethanol; ISOPROPYLAMIDE; N,N-dimethyl-formamide;