methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

Base Information

Chemical Name:methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate
CAS No.:1308255-29-9
Molecular Formula:C₁₆H₁₈BN₃O₆S
Molecular Weight:391.212
Hs Code.:

Synonyms:methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

Suppliers and Price of methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

There total 5 articles about methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.28%

: 1308254-86-5
4-amino-2-(aminomethyl)-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)benzenesulfonamide

: 79-22-1
methyl chloroformate

: 1308255-29-9
methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

: 1308255-31-3
methyl 3-((methoxycarbonylamino)methyl)-4-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

Guidance literature:: With pyridine; at 20 ℃;

Reference yield:

: 16588-02-6
4-chloro-3-cyanonitrobenzene

: 1308255-29-9
methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

: 1308255-31-3
methyl 3-((methoxycarbonylamino)methyl)-4-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetonitrile / 20 °C

2: acetic acid; chlorine / water / 2 h / 15 °C

3: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

4: hydrogen; ammonium hydroxide / water; methanol / 20 °C / Inert atmosphere

5: pyridine / 20 °C

With 4-methyl-morpholine; pyridine; ammonium hydroxide; hydrogen; chlorine; potassium carbonate; acetic acid; In methanol; water; acetonitrile;

Reference yield:

: 175135-67-8
2-(benzylthio)-5-nitrobenzonitrile

: 1308255-29-9
methyl 5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)benzylcarbamate

: 1308255-31-3
methyl 3-((methoxycarbonylamino)methyl)-4-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; chlorine / water / 2 h / 15 °C

2: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

3: hydrogen; ammonium hydroxide / water; methanol / 20 °C / Inert atmosphere

4: pyridine / 20 °C

With 4-methyl-morpholine; pyridine; ammonium hydroxide; hydrogen; chlorine; acetic acid; In methanol; water; acetonitrile;