N¹,N¹-diethyl-N⁴-[6-methoxy-2-(2,4,6-trichloro-styryl)-quinazolin-4-yl]-pentane-1,4-diamine

Base Information

• Chemical Name: N¹,N¹-diethyl-N⁴-[6-methoxy-2-(2,4,6-trichloro-styryl)-quinazolin-4-yl]-pentane-1,4-diamine
• CAS No.: 69258-60-2
• Molecular Formula: C₂₆H₃₁Cl₃N₄O
• Molecular Weight: 521.917

Synonyms:N¹,N¹-diethyl-N⁴-[6-methoxy-2-(2,4,6-trichloro-styryl)-quinazolin-4-yl]-pentane-1,4-diamine

Chemical Property of N¹,N¹-diethyl-N⁴-[6-methoxy-2-(2,4,6-trichloro-styryl)-quinazolin-4-yl]-pentane-1,4-diamine

Chemical Property:

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Technology Process of N¹,N¹-diethyl-N⁴-[6-methoxy-2-(2,4,6-trichloro-styryl)-quinazolin-4-yl]-pentane-1,4-diamine

There total 2 articles about N¹,N¹-diethyl-N⁴-[6-methoxy-2-(2,4,6-trichloro-styryl)-quinazolin-4-yl]-pentane-1,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

2,4,6-trichlorobenzaldehyde (24473-00-5) + 2-Methyl-4-(δ-diethylamino-α-methylbutylamino)-6-methoxyquinazoline (60395-93-9) → N1,N1-diethyl-N4-[6-methoxy-2-(2,4,6-trichloro-styryl)-quinazolin-4-yl]-pentane-1,4-diamine (69258-60-2)

Guidance literature:

With sodium acetate; In acetic anhydride; at 139 - 141 ℃; for 12h;

DOI:10.1007/BF00762032

Reference yield:

→ N1,N1-diethyl-N4-[6-methoxy-2-(2,4,6-trichloro-styryl)-quinazolin-4-yl]-pentane-1,4-diamine (69258-60-2)

Guidance literature:

4-<4-Diaethylamino-1-methyl-butylamino>-6-methoxy-2-methyl-chinazolin IIb, 2,4,6-Trichlor-benzaldehyd, Acetanhydrid / Na-Acetat;

DOI:10.1007/BF00772641

upstream raw materials:

2,4,6-trichlorobenzaldehyde

2-Methyl-4-(δ-diethylamino-α-methylbutylamino)-6-methoxyquinazoline

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