1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane

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Chemical Name:1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane
CAS No.:144191-94-6
Molecular Formula:C₂₅H₂₉NO₅
Molecular Weight:423.509
Hs Code.:

Synonyms:1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane

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Chemical Property of 1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane

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Technology Process of 1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane

There total 10 articles about 1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 143144-68-7
1-allyl-2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene

: 144191-94-6
1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; for 18h; Ambient temperature;
DOI:10.1021/jo00049a035

Reference yield:

: 143144-68-7
1-allyl-2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene

: 144299-23-0
(2S)-1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane

: 144191-94-6,144299-23-0
(2R)-1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane

: 144192-04-1
Carbonic acid tert-butyl ester 4-((S)-2,3-dihydroxy-propyl)-3-{[1-phenyl-meth-(E)-ylidene]-amino}-naphthalen-1-yl ester

: 144192-04-1
Carbonic acid tert-butyl ester 4-((R)-2,3-dihydroxy-propyl)-3-{[1-phenyl-meth-(E)-ylidene]-amino}-naphthalen-1-yl ester

Guidance literature:: With osmium(VIII) oxide; hydroquinuclidine 9-phenanthryl ether; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 18h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00049a035

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 144191-94-6
1,2-dihydroxy-3-<2-(benzylamino)-4-<<(tert-butyloxy)carbonyl>oxy>naphthalene-1-yl>propane

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 4-dimethylaminopyridine, 2) Na₂S₂O₄ / 1) CH₃CN, 18 h, RT, 2) H₂O, EtOAc, 24 h, RT

2: 84 percent / N-methylmorpholine N-oxide, OsO₄ / acetone; H₂O / 18 h / Ambient temperature

With dmap; osmium(VIII) oxide; sodium dithionite; 4-methylmorpholine N-oxide; In water; acetone;
DOI:10.1021/jo00049a035