(E)-S-ethyl 6-(2-(4-methoxybenzoyl)cyclopropyl)-2-methylhex-2-enethioate

Base Information

Chemical Name:(E)-S-ethyl 6-(2-(4-methoxybenzoyl)cyclopropyl)-2-methylhex-2-enethioate
CAS No.:1262862-74-7
Molecular Formula:C₂₀H₂₆O₃S
Molecular Weight:346.491
Hs Code.:

Synonyms:(E)-S-ethyl 6-(2-(4-methoxybenzoyl)cyclopropyl)-2-methylhex-2-enethioate

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Chemical Property of (E)-S-ethyl 6-(2-(4-methoxybenzoyl)cyclopropyl)-2-methylhex-2-enethioate

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Technology Process of (E)-S-ethyl 6-(2-(4-methoxybenzoyl)cyclopropyl)-2-methylhex-2-enethioate

There total 5 articles about (E)-S-ethyl 6-(2-(4-methoxybenzoyl)cyclopropyl)-2-methylhex-2-enethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1262863-26-2
4-(2-(4-methoxybenzoyl)cyclopropyl)butanal

: 127921-40-8
S-ethyl 2-(diethoxyphosphoryl)propanethioate

: 1262862-74-7
(E)-S-ethyl 6-(2-(4-methoxybenzoyl)cyclopropyl)-2-methylhex-2-enethioate

Guidance literature:: S-ethyl 2-(diethoxyphosphoryl)propanethioate; With sodium hydride; In 1,2-dimethoxyethane; for 0.5h; Inert atmosphere;

4-(2-(4-methoxybenzoyl)cyclopropyl)butanal; In 1,2-dimethoxyethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja107849y

Reference yield:

: 1262863-41-1
C₁₆H₂₂O₄

: 1262862-74-7
(E)-S-ethyl 6-(2-(4-methoxybenzoyl)cyclopropyl)-2-methylhex-2-enethioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / dimethyl sulfoxide / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: hydrogenchloride; water / tetrahydrofuran / 0.33 h

3.1: sodium hydride / 1,2-dimethoxyethane / 0.5 h / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

With hydrogenchloride; water; sodium hydride; In tetrahydrofuran; 1,2-dimethoxyethane; dimethyl sulfoxide;
DOI:10.1021/ja107849y

Reference yield:

: C₁₇H₂₄O₄

: 1262862-74-7
(E)-S-ethyl 6-(2-(4-methoxybenzoyl)cyclopropyl)-2-methylhex-2-enethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 0.33 h

2.1: sodium hydride / 1,2-dimethoxyethane / 0.5 h / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With hydrogenchloride; water; sodium hydride; In tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1021/ja107849y