C₂₇H₂₄N₄O₄S

Base Information

• Chemical Name: C₂₇H₂₄N₄O₄S
• CAS No.: 1361091-86-2
• Molecular Formula: C₂₇H₂₄N₄O₄S
• Molecular Weight: 500.578

Synonyms:C₂₇H₂₄N₄O₄S

Chemical Property of C₂₇H₂₄N₄O₄S

Chemical Property:

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Technology Process of C₂₇H₂₄N₄O₄S

There total 1 articles about C₂₇H₂₄N₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl (2-ethyl)propionylacetate (32493-32-6) → C27H24N4O4S (1361091-86-2)

Guidance literature:

Multi-step reaction with 8 steps

1.1: sodium hydroxide / ethanol; water / 10 h

1.2: 4 h / 0 - 20 °C / pH 7 - 8

1.3: Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 72 h / Inert atmosphere; Reflux

3.1: phenyltrimethylammonium tribromide / tetrahydrofuran / 1.5 h / Reflux

4.1: N,N-dimethyl-formamide / 12 h / Inert atmosphere

5.1: 2-mercaptoethylamine hydrochloride; sodium hydrogencarbonate / acetonitrile / 12 h

6.1: triethylamine / acetonitrile / 12 h / 20 °C / Inert atmosphere

7.1: 3-chloro-benzenecarboperoxoic acid / N,N-dimethyl-formamide / 12 h / -25 - 20 °C

8.1: ammonium acetate; acetic acid / 3 h / 180 °C / Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; 2-mercaptoethylamine hydrochloride; phenyltrimethylammonium tribromide; sodium hydrogencarbonate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/chem.201103001

upstream raw materials:

methyl (2-ethyl)propionylacetate

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