(2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide

Base Information

Chemical Name:(2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide
CAS No.:919529-48-9
Molecular Formula:C₂₃H₃₀N₄O₄
Molecular Weight:426.516
Hs Code.:

Synonyms:(2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide

Chemical Property:

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Technology Process of (2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide

There total 2 articles about (2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₁N₃O₃

: 100564-78-1,108524-68-1,142926-43-0,82732-07-8
(2R)-(tert-butoxycarbonylamino)-4-phenylbutanoic acid

: 919529-48-9
(2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide

Guidance literature:: C₂₃H₂₁N₃O₃; (2R)-(tert-butoxycarbonylamino)-4-phenylbutanoic acid; With HBTU; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 22 ℃; for 0.75h;

With diethylamine; In acetonitrile; for 0.3h; Product distribution / selectivity;

Reference yield:

: C₂HF₃O₂*C₂₃H₂₁N₃O₃

: 100564-78-1,108524-68-1,142926-43-0,82732-07-8
(2R)-(tert-butoxycarbonylamino)-4-phenylbutanoic acid

: 919529-48-9
(2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide

Guidance literature:: (2R)-(tert-butoxycarbonylamino)-4-phenylbutanoic acid; With HBTU; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 22 ℃; for 0.0833333h;

C₂HF₃O₂*C₂₃H₂₁N₃O₃; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 22 ℃; for 0.5h;

With diethylamine; In acetonitrile; for 0.3h; Product distribution / selectivity;

Reference yield: 37.5%

: 919529-48-9
(2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide

: 919527-90-5
N-amino-6-[(fluoren-9-ylmethoxy)carbonylamino]hexanamide trifluoroacetic acid salt

: 76-05-1
trifluoroacetic acid

: N-{[4-(N-{(2R)-2-[(tert-butoxy)carbonylamino]-4-phenylbutanoylamino}carbamoyl)phenyl]methyl}-6-aminohexanamide trifluoroacetic acid salt

Guidance literature:: (2R)-N-{[4-(aminomethyl)phenyl]carbonylamino}-2-[(tert-butoxy)carbonylamino]-4-phenylbutanamide; N-amino-6-[(fluoren-9-ylmethoxy)carbonylamino]hexanamide trifluoroacetic acid salt; With HBTU; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 22 ℃; for 0.75h;

With diethylamine; In acetonitrile; for 0.3h;

trifluoroacetic acid; In water; acetonitrile;