Trifluoro-acetic acid ((2R,4S)-4-methyl-tetrahydro-pyran-2-yl)-phenylsulfanyl-methyl ester

Base Information

Chemical Name:Trifluoro-acetic acid ((2R,4S)-4-methyl-tetrahydro-pyran-2-yl)-phenylsulfanyl-methyl ester
CAS No.:216865-99-5
Molecular Formula:C₁₅H₁₇F₃O₃S
Molecular Weight:334.359
Hs Code.:

Synonyms:Trifluoro-acetic acid ((2R,4S)-4-methyl-tetrahydro-pyran-2-yl)-phenylsulfanyl-methyl ester

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Chemical Property of Trifluoro-acetic acid ((2R,4S)-4-methyl-tetrahydro-pyran-2-yl)-phenylsulfanyl-methyl ester

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Technology Process of Trifluoro-acetic acid ((2R,4S)-4-methyl-tetrahydro-pyran-2-yl)-phenylsulfanyl-methyl ester

There total 4 articles about Trifluoro-acetic acid ((2R,4S)-4-methyl-tetrahydro-pyran-2-yl)-phenylsulfanyl-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 407-25-0
trifluoroacetic anhydride

: (2R,4S)-2-Benzenesulfinylmethyl-4-methyl-tetrahydro-pyran

: 216865-99-5
Trifluoro-acetic acid ((2R,4S)-4-methyl-tetrahydro-pyran-2-yl)-phenylsulfanyl-methyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; Yield given;
DOI:10.1016/S0040-4039(98)01795-X

Reference yield:

: 216865-98-4
(2R,4S)-4-Methyl-2-phenylsulfanylmethyl-tetrahydro-pyran

: 216865-99-5
Trifluoro-acetic acid ((2R,4S)-4-methyl-tetrahydro-pyran-2-yl)-phenylsulfanyl-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: mCPBA / CH₂Cl₂ / -78 °C

2: pyridine / CH₂Cl₂ / 0 °C

With pyridine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4039(98)01795-X

Reference yield:

: 216865-94-0
(4R,6R)-4-Methyl-6-phenylsulfanylmethyl-tetrahydro-pyran-2-ol

: 216865-99-5
Trifluoro-acetic acid ((2R,4S)-4-methyl-tetrahydro-pyran-2-yl)-phenylsulfanyl-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / Et₃SiH, BF₃*Et₂O / CH₂Cl₂ / -45 to 0 deg C

2: mCPBA / CH₂Cl₂ / -78 °C

3: pyridine / CH₂Cl₂ / 0 °C

With pyridine; triethylsilane; boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4039(98)01795-X