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C50H62O18

Base Information
  • Chemical Name:C50H62O18
  • CAS No.:1339943-42-8
  • Molecular Formula:C50H62O18
  • Molecular Weight:951.031
  • Hs Code.:
C<sub>50</sub>H<sub>62</sub>O<sub>18</sub>

Synonyms:C50H62O18

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Chemical Property of C50H62O18
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Technology Process of C50H62O18

There total 20 articles about C50H62O18 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 24h;
Guidance literature:
Multi-step reaction with 10 steps
1.1: phosgene / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C
1.2: 3.33 h / Reflux
2.1: sodium hydroxide / water / 20 °C / pH 7 / Aqueous phosphate buffer
3.1: potassium iodide; sodium hydrogencarbonate; iodine / water / 24 h / 0 - 20 °C
4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 h / Reflux
5.1: sodium hydrogencarbonate / 12 h / 20 °C / Inert atmosphere
6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h
7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 17 h / 10 - 20 °C
8.1: methyllithium; boron trifluoride diethyl etherate; copper(l) cyanide / diethyl ether; tetrahydrofuran / -78 °C
9.1: dichloromethane / 2 h / 20 °C / Molecular sieve; Inert atmosphere
9.2: 0.25 h
9.3: 2 h / Inert atmosphere
10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C
With phosgene; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; methyllithium; iodine; copper(l) cyanide; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; potassium iodide; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; dichloromethane; water;
Guidance literature:
Multi-step reaction with 11 steps
1.1: sodium hydroxide / water / 20 °C / pH 7 / Aqueous phosphate buffer
2.1: phosgene / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C
2.2: 3.33 h / Reflux
3.1: sodium hydroxide / water / 20 °C / pH 7 / Aqueous phosphate buffer
4.1: potassium iodide; sodium hydrogencarbonate; iodine / water / 24 h / 0 - 20 °C
5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 20 h / Reflux
6.1: sodium hydrogencarbonate / 12 h / 20 °C / Inert atmosphere
7.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h
8.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 17 h / 10 - 20 °C
9.1: methyllithium; boron trifluoride diethyl etherate; copper(l) cyanide / diethyl ether; tetrahydrofuran / -78 °C
10.1: dichloromethane / 2 h / 20 °C / Molecular sieve; Inert atmosphere
10.2: 0.25 h
10.3: 2 h / Inert atmosphere
11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C
With phosgene; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; methyllithium; iodine; copper(l) cyanide; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; potassium iodide; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; dichloromethane; water;
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