Technology Process of (Os(N2C10H8)2(C6H4CONC6H5))(1+)*ClO4(1-)=(Os(N2C10H8)2(C6H4CONC6H5))(ClO4)
There total 1 articles about (Os(N2C10H8)2(C6H4CONC6H5))(1+)*ClO4(1-)=(Os(N2C10H8)2(C6H4CONC6H5))(ClO4) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
Na2CO3;
In
2-methoxy-ethanol; water;
to mixt. N-phenylbenzohydroxamic acid and Na2CO3 were added 2-methoxyethanol and (Os(bpy)2Br2) and heated at reflux for 72 h under N2 atm., soln. was cooled to room temp., aq. soln. NaClO4 was added; ppt. was filtered, washed with water and dried in air, recrystn. from CH2Cl2-benzene;
DOI:10.1021/ic0012569