N-cyclohexyl-4-((((2S,3S)-3-hydroxy-2,6-dimethylheptyl)oxy)methyl)-N-methylbenzene sulfonamide

Base Information

Chemical Name:N-cyclohexyl-4-((((2S,3S)-3-hydroxy-2,6-dimethylheptyl)oxy)methyl)-N-methylbenzene sulfonamide
CAS No.:1574549-93-1
Molecular Formula:C₂₃H₃₉NO₄S
Molecular Weight:425.633
Hs Code.:

Synonyms:N-cyclohexyl-4-((((2S,3S)-3-hydroxy-2,6-dimethylheptyl)oxy)methyl)-N-methylbenzene sulfonamide

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Chemical Property of N-cyclohexyl-4-((((2S,3S)-3-hydroxy-2,6-dimethylheptyl)oxy)methyl)-N-methylbenzene sulfonamide

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Technology Process of N-cyclohexyl-4-((((2S,3S)-3-hydroxy-2,6-dimethylheptyl)oxy)methyl)-N-methylbenzene sulfonamide

There total 4 articles about N-cyclohexyl-4-((((2S,3S)-3-hydroxy-2,6-dimethylheptyl)oxy)methyl)-N-methylbenzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133718-19-1
4-(bromomethyl)-N-cyclohexyl-N-methylbenzenesulfonamide

: (2S,3S)-2,6-dimethylheptane-1,3-diol

: 1574549-93-1
N-cyclohexyl-4-((((2S,3S)-3-hydroxy-2,6-dimethylheptyl)oxy)methyl)-N-methylbenzene sulfonamide

Guidance literature:: (2S,3S)-2,6-dimethylheptane-1,3-diol; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 0.333333h; Inert atmosphere;

4-(bromomethyl)-N-cyclohexyl-N-methylbenzenesulfonamide; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.01.003

Reference yield:

: 1119-16-0
isocaproic aldehyde

: 1574549-93-1
N-cyclohexyl-4-((((2S,3S)-3-hydroxy-2,6-dimethylheptyl)oxy)methyl)-N-methylbenzene sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C

1.2: 2.5 h / -78 - 20 °C

1.3: 1 h / 20 °C

2.1: lithium borohydride / diethyl ether; water / 1 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

With lithium borohydride; di-n-butylboryl trifluoromethanesulfonate; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.01.003

Reference yield:

: (R)-4-benzyl-3-[(2R,3S)-3-hydroxy-2,6-dimethylheptanoyl]-1,3-oxazolidin-2-one

: 1574549-93-1
N-cyclohexyl-4-((((2S,3S)-3-hydroxy-2,6-dimethylheptyl)oxy)methyl)-N-methylbenzene sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium borohydride / diethyl ether; water / 1 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With lithium borohydride; sodium hydride; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.01.003