2-ethenyl-N-phenylbenzamide

Base Information

Chemical Name:2-ethenyl-N-phenylbenzamide
CAS No.:27326-46-1
Molecular Formula:C₁₅H₁₃NO
Molecular Weight:223.274
Hs Code.:
DSSTox Substance ID:DTXSID901309896
Nikkaji Number:J1.334.268G

Synonyms:2-ethenyl-N-phenylbenzamide;SCHEMBL2255814;DTXSID901309896;27326-46-1

Suppliers and Price of 2-ethenyl-N-phenylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-ethenyl-N-phenylbenzamide

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:223.099714038
Heavy Atom Count:17
Complexity:268

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CC1=CC=CC=C1C(=O)NC2=CC=CC=C2

Technology Process of 2-ethenyl-N-phenylbenzamide

There total 6 articles about 2-ethenyl-N-phenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 28269-50-3
2-vinylbenzoic acid chloride

: 62-53-3
aniline

: 27326-46-1
N-phenyl-2-vinylbenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 6h;
DOI:10.1002/adsc.202000260

Reference yield: 47.0%

: 27326-43-8
2-vinylbenzoic acid

: 62-53-3
aniline

: 27326-46-1
N-phenyl-2-vinylbenzamide

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 23 ℃; for 6h;
DOI:10.1021/acs.orglett.9b04233

Reference yield:

: 119-67-5
o-carboxybenzaldehyde

: 27326-46-1
N-phenyl-2-vinylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: Reflux

2.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 2 h / 60 °C

3.1: triethylamine / dichloromethane / 6 h / 0 - 20 °C

With thionyl chloride; potassium tert-butylate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201700369