10-methoxy-3-methyl-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl 3-fluorobenzenesulfonate

Base Information

Chemical Name:10-methoxy-3-methyl-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl 3-fluorobenzenesulfonate
CAS No.:1233353-89-3
Molecular Formula:C₂₅H₂₄FNO₄S
Molecular Weight:453.534
Hs Code.:

Synonyms:10-methoxy-3-methyl-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl 3-fluorobenzenesulfonate

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Chemical Property of 10-methoxy-3-methyl-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl 3-fluorobenzenesulfonate

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Technology Process of 10-methoxy-3-methyl-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl 3-fluorobenzenesulfonate

There total 2 articles about 10-methoxy-3-methyl-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl 3-fluorobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1233354-89-6
C₂₅H₂₆FNO₆S

: 1233353-89-3
10-methoxy-3-methyl-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl 3-fluorobenzenesulfonate

Guidance literature:: C₂₅H₂₆FNO₆S; With trichlorophosphate; In toluene; at 20 ℃; Reflux;

With methanol; sodium tetrahydroborate; at 0 ℃; for 0.166667h;

Reference yield:

: 1233354-60-3
7-methoxy-3-oxo-3,4-dihydro-1H-2-benzopyran-8-yl 3-fluorobenzene-1-sulfonate

: 55755-17-4
2-(3-methylphenyl)ethylamine

: 1233353-89-3
10-methoxy-3-methyl-5,6,7,8,13,13a-hexahydroisoquinolino[2,1-b]isoquinolin-9-yl 3-fluorobenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / methanol / Reflux

2.1: trichlorophosphate / toluene / 2 h / Reflux

2.2: 0.17 h / 0 °C

With triethylamine; trichlorophosphate; In methanol; toluene;