(3E,8E)-1,6-Bis-(2,4,6-triisopropyl-benzenesulfonyl)-1,2,5,6,7,10-hexahydro-[1,6]diazecine

Base Information

Chemical Name:(3E,8E)-1,6-Bis-(2,4,6-triisopropyl-benzenesulfonyl)-1,2,5,6,7,10-hexahydro-[1,6]diazecine
CAS No.:219839-26-6
Molecular Formula:C₃₈H₅₈N₂O₄S₂
Molecular Weight:671.022
Hs Code.:

Synonyms:(3E,8E)-1,6-Bis-(2,4,6-triisopropyl-benzenesulfonyl)-1,2,5,6,7,10-hexahydro-[1,6]diazecine

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Chemical Property of (3E,8E)-1,6-Bis-(2,4,6-triisopropyl-benzenesulfonyl)-1,2,5,6,7,10-hexahydro-[1,6]diazecine

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Technology Process of (3E,8E)-1,6-Bis-(2,4,6-triisopropyl-benzenesulfonyl)-1,2,5,6,7,10-hexahydro-[1,6]diazecine

There total 17 articles about (3E,8E)-1,6-Bis-(2,4,6-triisopropyl-benzenesulfonyl)-1,2,5,6,7,10-hexahydro-[1,6]diazecine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 105536-22-9
2,4,6-triisopropylbenzene sulfonamide

: 219838-95-6
(Z)-but-2-ene-1,4-bis(ethylcarbonate)

: 219839-30-2
(E,E,E,E)-1,6,11,16-tetrakis[(2,4,6-triisopropylphenyl)sulfonyl]-1,6,11,16-tetraazacycloicosa-3,8,13,18-tetraene

: 219839-26-6
(3E,8E)-1,6-Bis-(2,4,6-triisopropyl-benzenesulfonyl)-1,2,5,6,7,10-hexahydro-[1,6]diazecine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 72h; Ambient temperature;
DOI:10.1016/S0040-4020(98)00931-4

Reference yield: 1.5%

: 105536-22-9
2,4,6-triisopropylbenzene sulfonamide

: 219838-95-6
(Z)-but-2-ene-1,4-bis(ethylcarbonate)

: 219839-28-8
(E,E,E)-1,6,11-tris[(2,4,6-triisopropylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene

: C₆₃H₉₇N₃O₁₁S₃

: 219839-30-2
(E,E,E,E)-1,6,11,16-tetrakis[(2,4,6-triisopropylphenyl)sulfonyl]-1,6,11,16-tetraazacycloicosa-3,8,13,18-tetraene

: 219839-26-6
(3E,8E)-1,6-Bis-(2,4,6-triisopropyl-benzenesulfonyl)-1,2,5,6,7,10-hexahydro-[1,6]diazecine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 0 ℃; for 24h; Further byproducts given;
DOI:10.1016/S0040-4020(98)00931-4

Reference yield: 1.5%

: 105536-22-9
2,4,6-triisopropylbenzene sulfonamide

: 219838-95-6
(Z)-but-2-ene-1,4-bis(ethylcarbonate)

: C₁₀₁H₁₅₅N₅O₁₅S₅

: 219839-28-8
(E,E,E)-1,6,11-tris[(2,4,6-triisopropylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triene

: 219839-30-2
(E,E,E,E)-1,6,11,16-tetrakis[(2,4,6-triisopropylphenyl)sulfonyl]-1,6,11,16-tetraazacycloicosa-3,8,13,18-tetraene

: 219839-26-6
(3E,8E)-1,6-Bis-(2,4,6-triisopropyl-benzenesulfonyl)-1,2,5,6,7,10-hexahydro-[1,6]diazecine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 0 ℃; for 24h; Further byproducts given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4020(98)00931-4