Technology Process of perloline
There total 13 articles about perloline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium bis(2-methoxyethoxy)aluminium dihydride;
In
tetrahydrofuran;
for 0.0333333h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 43 percent / AcOH, 11M HCl / H2O / 2 h / Heating
2: 1.) 75percent H2SO4, 2.) NaNO2 / 1.) 80-100 deg C, 2h, 2.) 2h
3: 87 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 39 h / Ambient temperature
4: 86 percent / lithium hexamethyldisilazide / tetrahydrofuran / 96 h / Heating
5: 70 percent / sodium bis(methoxyethoxy)aluminium hydride / tetrahydrofuran / 0.03 h
With
hydrogenchloride; sulfuric acid; acetic acid; dicyclohexyl-carbodiimide; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium hexamethyldisilazane; sodium nitrite;
In
tetrahydrofuran; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) 75percent H2SO4, 2.) NaNO2 / 1.) 80-100 deg C, 2h, 2.) 2h
2: 87 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 39 h / Ambient temperature
3: 86 percent / lithium hexamethyldisilazide / tetrahydrofuran / 96 h / Heating
4: 70 percent / sodium bis(methoxyethoxy)aluminium hydride / tetrahydrofuran / 0.03 h
With
sulfuric acid; dicyclohexyl-carbodiimide; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium hexamethyldisilazane; sodium nitrite;
In
tetrahydrofuran;
