Thiocarbonic acid O-((1R,2R,5R)-2,5-diphenyl-cyclohexyl) ester O-phenyl ester

Base Information

• Chemical Name: Thiocarbonic acid O-((1R,2R,5R)-2,5-diphenyl-cyclohexyl) ester O-phenyl ester
• CAS No.: 93783-01-8
• Molecular Formula: C₂₅H₂₄O₂S
• Molecular Weight: 388.53

Synonyms:Thiocarbonic acid O-((1R,2R,5R)-2,5-diphenyl-cyclohexyl) ester O-phenyl ester

Chemical Property of Thiocarbonic acid O-((1R,2R,5R)-2,5-diphenyl-cyclohexyl) ester O-phenyl ester

Chemical Property:

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Technology Process of Thiocarbonic acid O-((1R,2R,5R)-2,5-diphenyl-cyclohexyl) ester O-phenyl ester

There total 2 articles about Thiocarbonic acid O-((1R,2R,5R)-2,5-diphenyl-cyclohexyl) ester O-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

c-2,c-5-diphenylcyclohexan-r-1-ol (93782-98-0) + phenylcarbonochloridothioate (1005-56-7) → Thiocarbonic acid O-((1R,2R,5R)-2,5-diphenyl-cyclohexyl) ester O-phenyl ester (93783-01-8)

Guidance literature:

With dmap; In dichloromethane; at 25 ℃; for 18h;

DOI:10.1021/jo00203a023

Reference yield:

Acetic acid (1R,2R,5R)-2,5-diphenyl-cyclohexyl ester (93782-99-1) → Thiocarbonic acid O-((1R,2R,5R)-2,5-diphenyl-cyclohexyl) ester O-phenyl ester (93783-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / ethanol / 21 h / 25 °C

2: 97 percent / 4-dimethylaminopyridine / CH₂Cl₂ / 18 h / 25 °C

With dmap; potassium hydroxide; In ethanol; dichloromethane;

DOI:10.1021/jo00203a023

Reference yield: 53.0%

Thiocarbonic acid O-((1R,2R,5R)-2,5-diphenyl-cyclohexyl) ester O-phenyl ester (93783-01-8) → (Z)-1,4-diphenylcyclohexane (21072-41-3)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 13h; Heating;

DOI:10.1021/jo00203a023

upstream raw materials:

c-2,c-5-diphenylcyclohexan-r-1-ol

phenylcarbonochloridothioate

Acetic acid (1R,2R,5R)-2,5-diphenyl-cyclohexyl ester

Downstream raw materials:

(Z)-1,4-diphenylcyclohexane

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