4-(3,3-dimethyl-2-oxobutyl)-N-(3,5-dimethylphenyl)piperazine-1-carboxamide

Base Information

Chemical Name:4-(3,3-dimethyl-2-oxobutyl)-N-(3,5-dimethylphenyl)piperazine-1-carboxamide
CAS No.:1195786-21-0
Molecular Formula:C₁₉H₂₉N₃O₂
Molecular Weight:331.458
Hs Code.:

Synonyms:4-(3,3-dimethyl-2-oxobutyl)-N-(3,5-dimethylphenyl)piperazine-1-carboxamide

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Chemical Property of 4-(3,3-dimethyl-2-oxobutyl)-N-(3,5-dimethylphenyl)piperazine-1-carboxamide

Chemical Property:

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Technology Process of 4-(3,3-dimethyl-2-oxobutyl)-N-(3,5-dimethylphenyl)piperazine-1-carboxamide

There total 3 articles about 4-(3,3-dimethyl-2-oxobutyl)-N-(3,5-dimethylphenyl)piperazine-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1225543-19-0
C₁₃H₁₉N₃O

: 5469-26-1
1-Bromopinacolon

: 1195786-21-0
4-(3,3-dimethyl-2-oxobutyl)-N-(3,5-dimethylphenyl)piperazine-1-carboxamide

Guidance literature:: With polystyrene-bound N-methylmorpholine; In N,N-dimethyl-formamide; at 75 ℃; for 0.1h;
DOI:10.1021/ol902101c

Reference yield:

: 54132-75-1
3,5-dimethylphenyl isocyanate

: 1195786-21-0
4-(3,3-dimethyl-2-oxobutyl)-N-(3,5-dimethylphenyl)piperazine-1-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 100 °C / Flow reactor; Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 80 °C / Inert atmosphere; Flow reactor

3: polystyrene-N-methylmorpholine column / N,N-dimethyl-formamide / 75 °C / Flow reactor

With palladium 10% on activated carbon; hydrogen; In N,N-dimethyl-formamide;
DOI:10.1002/chem.201204350

Reference yield:

: C₂₁H₂₅N₃O₃

: 1195786-21-0
4-(3,3-dimethyl-2-oxobutyl)-N-(3,5-dimethylphenyl)piperazine-1-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / N,N-dimethyl-formamide / 80 °C / Inert atmosphere; Flow reactor

2: polystyrene-N-methylmorpholine column / N,N-dimethyl-formamide / 75 °C / Flow reactor

With palladium 10% on activated carbon; hydrogen; In N,N-dimethyl-formamide;
DOI:10.1002/chem.201204350