(9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate

Base Information

Chemical Name:(9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate
CAS No.:1327157-41-4
Molecular Formula:C₂₄H₂₁N₅O₂S
Molecular Weight:443.529
Hs Code.:

Synonyms:(9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate

Suppliers and Price of (9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of (9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate

There total 3 articles about (9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1327157-24-3
(9H-fluoren-9-yl)methyl (S)-1-phenyl-2-thiocyanatoethylcarbamate

: 1327157-41-4
(9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate

Guidance literature:: With sodium azide; zinc dibromide; In water; isopropyl alcohol; Reflux;
DOI:10.1055/s-0030-1259972

Reference yield:

: 1172596-36-9
Fmoc-Phg-ψ[CH2I]

: 1327157-41-4
(9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide / tetrahydrofuran / 3 h / Reflux

2: sodium azide; zinc dibromide / water; isopropyl alcohol / Reflux

With sodium azide; tetrabutylammomium bromide; zinc dibromide; In tetrahydrofuran; water; isopropyl alcohol;
DOI:10.1055/s-0030-1259972

Reference yield:

: 215178-44-2
(2-hydroxy-1-phenylethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

: 1327157-41-4
(9H-fluoren-9-yl)methyl (S)-1-phenyl-2-(2H-tetrazol-5-ylthio)ethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole; iodine; triphenylphosphine

2: tetrabutylammomium bromide / tetrahydrofuran / 3 h / Reflux

3: sodium azide; zinc dibromide / water; isopropyl alcohol / Reflux

With 1H-imidazole; sodium azide; tetrabutylammomium bromide; iodine; triphenylphosphine; zinc dibromide; In tetrahydrofuran; water; isopropyl alcohol; 1: Mitsunobu reaction;
DOI:10.1055/s-0030-1259972