C,C'-diphenyl-C,C'-(8-methyl-1,3,4,7-tetraphenyl-4,7-dihydro-4,7-epiazano-benzo[c]thiophene-5,6-diyl)-bis-methanone

Base Information

• Chemical Name: C,C'-diphenyl-C,C'-(8-methyl-1,3,4,7-tetraphenyl-4,7-dihydro-4,7-epiazano-benzo[c]thiophene-5,6-diyl)-bis-methanone
• CAS No.: 41223-61-4
• Molecular Formula: C₄₇H₃₃NO₂S
• Molecular Weight: 675.851

Synonyms:C,C'-diphenyl-C,C'-(8-methyl-1,3,4,7-tetraphenyl-4,7-dihydro-4,7-epiazano-benzo[c]thiophene-5,6-diyl)-bis-methanone

Chemical Property of C,C'-diphenyl-C,C'-(8-methyl-1,3,4,7-tetraphenyl-4,7-dihydro-4,7-epiazano-benzo[c]thiophene-5,6-diyl)-bis-methanone

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Technology Process of C,C'-diphenyl-C,C'-(8-methyl-1,3,4,7-tetraphenyl-4,7-dihydro-4,7-epiazano-benzo[c]thiophene-5,6-diyl)-bis-methanone

There total 3 articles about C,C'-diphenyl-C,C'-(8-methyl-1,3,4,7-tetraphenyl-4,7-dihydro-4,7-epiazano-benzo[c]thiophene-5,6-diyl)-bis-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dibenzoyl-1-methyl-2,5-diphenyl-pyrrole (18983-23-8) → C,C'-diphenyl-C,C'-(8-methyl-1,3,4,7-tetraphenyl-4,7-dihydro-4,7-epiazano-benzo[c]thiophene-5,6-diyl)-bis-methanone (41223-61-4)

Guidance literature:

Multi-step reaction with 2 steps

1: P₂S₅, Py

2: benzene

With pyridine; tetraphosphorus decasulfide; In benzene;

DOI:10.1021/ja00789a091

Reference yield:

5-methyl-1,3,4,6-tetraphenyl-1H-thieno[3,4-c]pyrrolium betaine (38336-72-0) + 1,4-diphenyl-but-2-yne-1,4-dione (1087-09-8) → C,C'-diphenyl-C,C'-(8-methyl-1,3,4,7-tetraphenyl-4,7-dihydro-4,7-epiazano-benzo[c]thiophene-5,6-diyl)-bis-methanone (41223-61-4)

Guidance literature:

In benzene;

DOI:10.1021/ja00789a091

Reference yield:

→ C,C'-diphenyl-C,C'-(8-methyl-1,3,4,7-tetraphenyl-4,7-dihydro-4,7-epiazano-benzo[c]thiophene-5,6-diyl)-bis-methanone (41223-61-4)

Guidance literature:

5, Dibenzoylidenacetylen;

DOI:10.1021/ja00813a027

upstream raw materials:

5-methyl-1,3,4,6-tetraphenyl-1H-thieno[3,4-c]pyrrolium betaine

1,4-diphenyl-but-2-yne-1,4-dione

3,4-dibenzoyl-1-methyl-2,5-diphenyl-pyrrole

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