5-[3-((1S,2S)-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester TBS hydrazone

Base Information

• Chemical Name: 5-[3-((1S,2S)-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester TBS hydrazone
• CAS No.: 1042168-25-1
• Molecular Formula: C₄₀H₅₈N₂O₄SSi
• Molecular Weight: 691.063

Synonyms:5-[3-((1S,2S)-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester TBS hydrazone

Chemical Property of 5-[3-((1S,2S)-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester TBS hydrazone

Chemical Property:

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Technology Process of 5-[3-((1S,2S)-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester TBS hydrazone

There total 1 articles about 5-[3-((1S,2S)-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester TBS hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-[3-((1S,2S)-2-{4-[1-(4-Methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester (956017-51-9) + 1,2-bis(tert-butyldimethylsilyl)hydrazine (10000-20-1) → 5-[3-((1S,2S)-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester TBS hydrazone (1042168-25-1)

Guidance literature:

scandium tris(trifluoromethanesulfonate); In chloroform; acetonitrile; at 0 - 20 ℃;

Reference yield: 50.0%

5-[3-((1S,2S)-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester TBS hydrazone (1042168-25-1) → C34H41BrO4S (1042168-80-8)

Guidance literature:

With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; bromine; In dichloromethane; at -78 - 20 ℃;

Reference yield: 49.0%

5-[3-((1S,2S)-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester TBS hydrazone (1042168-25-1) → 5-[3-((1S,2S)-3,3-Dichloro-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester (956017-55-3)

Guidance literature:

With triethylamine; copper dichloride; In methanol; chloroform; for 1h;

upstream raw materials:

5-[3-((1S,2S)-2-{4-[1-(4-Methoxy-benzyloxy)-hexyl]-phenyl}-3-oxo-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester

1,2-bis(tert-butyldimethylsilyl)hydrazine

Downstream raw materials:

5-[3-((1S,2S)-3,3-Dichloro-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester

C₃₄H₄₁BrO₄S

5-[3-((1S,2S)-3,3-dibromo-2-{4-[1-(4-methoxy-benzyloxy)-hexyl]-phenyl}-cyclopentyl)-propyl]-thiophene-2-carboxylic acid methyl ester

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