methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate

Base Information

Chemical Name:methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate
CAS No.:1402422-13-2
Molecular Formula:C₄₃H₅₂Cl₃NO₁₆S
Molecular Weight:977.308
Hs Code.:

methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate

Synonyms:methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate

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Chemical Property of methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate

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Technology Process of methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate

There total 1 articles about methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 630-18-2
tert-butyl isocyanide

: methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranose)uronate

: 1402422-13-2
methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1002/chem.201201041

Reference yield: 67.0%

: 1161723-22-3
C₂₃H₃₀O₈S

: 1402422-13-2
methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate

: 1402422-14-3
methyl-(2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-α-D-glucopyranosyl)-(1→4)-[methyl-(2-O-acetyl-3-O-methyl-α-L-idopyranosyl)uronate]-(1→4)-2,3-di-O-benzyl-6-deoxy-6-C-methoxysulfonylmethyl-α-D-glucopyranoside

Guidance literature:: C₂₃H₃₀O₈S; methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate; In dichloromethane; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 1h;
DOI:10.1002/chem.201201041

Reference yield: 63.0%

: 1161723-22-3
C₂₃H₃₀O₈S

: 1402422-13-2
methyl [2,3-di-O-benzyl-6-deoxy-6-C-ethoxysulfonylmethyl-4-O-(4-methoxybenzyl)-α-D-glucopyranosyl]-(1→?4)-(2-O-acetyl-3-O-methyl-α,β-L-idopyranosyl-1-trichloroacetimidate)uronate

: methyl [ethyl (2,3-di-O-benzyl-6-deoxy-6-C-sulfonatomethyl-α-D-glucopyranosyl)]-(1→4)-[methyl (2-O-acetyl-3-O-methyl-α-L-idopyranosyl)-uronate]-(1→4)-[sodium (2,3-di-O-benzyl-6-deoxy-6-C-sulfonatomethyl-α-D-glucopyranoside)]

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 0 ℃; for 2h; Molecular sieve;
DOI:10.1002/cmdc.202000917