(S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide

Base Information

Chemical Name:(S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide
CAS No.:116729-86-3
Molecular Formula:C₁₃H₁₈N₂O₄S
Molecular Weight:298.363
Hs Code.:

Synonyms:(S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide

Suppliers and Price of (S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide

Chemical Property:

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Technology Process of (S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide

There total 3 articles about (S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 109-87-5
Dimethoxymethane

: 116729-84-1
(S)-N-(1-cyano-3-hydroxypropan-2-yl)-p-toluenesulfonamide

: 116729-86-3
(S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide

Guidance literature:: With molecular sieve; phosphorus pentoxide; In dichloromethane; for 120h; Ambient temperature;
DOI:10.1002/hlca.19880710402

Reference yield:

: 59642-37-4
N-(p-toluenesulfonyl)L-asparagine methyl ester

: 116729-86-3
(S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / ClCOOCCl₃ / various solvent(s) / 0.17 h / 60 °C

2: 90 percent / NaBH₄ / methanol / 0.17 h / Heating

3: 87 percent / P₂O₅, molecular sieves / CH₂Cl₂ / 120 h / Ambient temperature

With sodium tetrahydroborate; molecular sieve; phosphorus pentoxide; trichloromethyl chloroformate; In methanol; dichloromethane;
DOI:10.1002/hlca.19880710402

Reference yield:

: 116729-82-9
(S)-methyl 3-cyano-2-<(p-toluenesulfonyl)amino>propionate

: 116729-86-3
(S)-N-<1-cyano-3-(methoxymethoxy)propan-2-yl>-p-toluenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaBH₄ / methanol / 0.17 h / Heating

2: 87 percent / P₂O₅, molecular sieves / CH₂Cl₂ / 120 h / Ambient temperature

With sodium tetrahydroborate; molecular sieve; phosphorus pentoxide; In methanol; dichloromethane;
DOI:10.1002/hlca.19880710402