PhMe₂GeNMe₂

Base Information

Chemical Name:PhMe₂GeNMe₂
CAS No.:1151774-02-5
Molecular Formula:C₁₀H₁₇GeN
Molecular Weight:223.842
Hs Code.:

Synonyms:PhMe₂GeNMe₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of PhMe₂GeNMe₂

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Technology Process of PhMe₂GeNMe₂

There total 1 articles about PhMe₂GeNMe₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3585-33-9
lithium dimethylamide

: 22702-76-7
phenyldimethylchlorogermane

: 1151774-02-5
PhMe₂GeNMe₂

Guidance literature:: In diethyl ether; byproducts: LiCl; (inert atm.); addn. of a soln. of amide in Et2O to a soln. of Ge compd. in Et2O, stirring for 18 h; evapn., dissolving in hexane, filtration through Celite, evapn.; elem. anal.;
DOI:10.1021/om900035r

Reference yield: 82.0%

: 1151774-02-5
PhMe₂GeNMe₂

: 2875-92-5
phenylgermane

: 32284-93-8
C₃₀H₃₈Ge₄

Guidance literature:: In acetonitrile; for 72h; Inert atmosphere; Schlenk technique; Glovebox; Heating;
DOI:10.1016/j.jorganchem.2017.07.021

Reference yield: 76.0%

: 1151774-02-5
PhMe₂GeNMe₂

: 2816-43-5
triphenylgermane

: 75-05-8,26809-02-9
acetonitrile

: 53445-88-8
PhMe₂GeGePh₃

Guidance literature:: In acetonitrile; byproducts: (CH3)2NH; (inert atm.); addn. of a soln. of Ph3GeH in acetonitrile to a soln. of Ge amide in acetonitrile, heating at 85°C for 96 h; evapn. in vac., distn. (120°C, 0.05 Torr); elem. anal.;
DOI:10.1021/om900035r